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I suggest an even better experiment: listening to Echoes (the wonderful song from the album Meddle, my favorite song btw) synched with 2001's last 24 minutes. You start the music as soon as those words - I belive it's "Jupter and beyond infinite" or something like that - appear onscreen. The music synchs perfectly to the stargate sequence and to the "hotel room" scene, and it ends exactly the same time as the movie. A very psychedelic experience, I did it only once (I own the album, but I don't have a 2001 copy anymore), and it was awesome.
i have also done this... in fact i have the clip on my computer set up with the music perfectly.... start the song when the title "Jupiter - and Beyond the Infinite" appears on your screen like ricarleite said. then just sit back and enjoy.... its creepy how well the two match up...
i particulary enjoy the guitar solo in the song... this is when he's sorda peaking out in the space ship... flying over (sorda looks like mountains) of all different colours... lol its awesome!